Picometer Scale Differences of Lattice Spacing In TEM Images

نویسنده

  • Martin Rose
چکیده

There are many applications in modern science in which a very precise knowledge of atom spacings i.e. lattice parameters is crucial. These include multi layer hetero structures in device manufacturing and core-rim nano particles, for example. In general it is interesting to know the change in spacings – or the strain in the proximity of a lattice defect or a coherent interface between two different substances. From the knowledge of the spacings e.g. relaxation processes can be studied. Mathematical transforms intermediate between direct and reciprocal space make possible digital darkfield strategies for mapping strain relaxation around interfaces and dislocations [1-5]. Here we examine applications to the measurement of lattice parameter differences between adjacent phases.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Dithiocarbamate-protected ruthenium nanoparticles: Synthesis, spectroscopy, electrochemistry and STM studies

Stable ruthenium nanoparticles were synthesized in a biphasic system with a protecting monolayer of dithiocarbamate derivatives. The core ize of the resulting Ru particles was found to vary with the initial ligand–metal feed ratio. UV–vis spectroscopic measurements showed a Mie cattering profile, with no obvious surface-plasmon resonance. The size and crystal structures of the particles were ch...

متن کامل

Quantitative TEM analysis of a hexagonal mesoporous silicate structure.

TEM analysis of mesoporous materials is generally undertaken to give qualitative results. Accurate quantitative analysis is demonstrated in this study. A systematic image analysis of a powder form of a hexagonal mesoporous material known as KIT-6 is conducted using a transmission electron microscope (TEM). Three types of image contrast typically appear in this material (a hexagonal honeycomb st...

متن کامل

بررسی اثر دمای بازپخت بر میکروکرنش‌های شبکه‌ی نانو ذرات اکسید قلع تهیه شده به روش سل- ژل

SnO2 nanoparticles have been synthesized via sol-gel method in different annealing temperatures. TEM, FESEM and XRD techniques have been used to investigate the structure and morphology of SnO2 nanoparticles. The XRD pattern analysis shows all samples are single phase. XRD patterns show as the annealing temperature increases, the peaks become sharper which is related to the increase in the crys...

متن کامل

Reduction of lattice thermal conductivity from planar faults in the layered Zintl compound SrZnSb2

The layered Zintl compound SrZnSb2 is investigated using transmission electron microscopy (TEM) to understand the low lattice thermal conductivity. The material displays out-of-phase boundaries with a spacing from 100 down to 2 nm. Density functional theory calculations confirm that the TEM-derived defect structure is energetically reasonable. The impact of these defects on phonon scattering is...

متن کامل

Novel role for vinculin in ventricular myocyte mechanics and dysfunction.

Vinculin (Vcl) plays a key structural role in ventricular myocytes that, when disrupted, can lead to contractile dysfunction and dilated cardiomyopathy. To investigate the role of Vcl in myocyte and myocardial function, cardiomyocyte-specific Vcl knockout mice (cVclKO) and littermate control wild-type mice were studied with transmission electron microscopy (TEM) and in vivo magnetic resonance i...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:

دوره   شماره 

صفحات  -

تاریخ انتشار 2006